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[求助]
求助,有機(jī)無機(jī)雜化碘酸鹽,結(jié)構(gòu)已明確只差最后的精修 已有1人參與
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各位專家好,這里有一個(gè)數(shù)據(jù)是有機(jī)無機(jī)雜化的碘酸鹽,結(jié)構(gòu)已經(jīng)明確,具體數(shù)據(jù)見網(wǎng)盤。鏈接:https://pan.baidu.com/s/1Uk7hpaXEOmhKyXX9xVGpPg?pwd=xhya 提取碼:xhya 需求如下: 我自己解析的話能力有限,僅能到此為止,系統(tǒng)提示氧可能有無序。我的目標(biāo)是盡量按照不無序?qū)⒅笜?biāo)修下來,無AB類錯(cuò)誤即可。 但如果確實(shí)要進(jìn)行無序處理 也是可以的 只是我在到時(shí)進(jìn)行結(jié)構(gòu)描述時(shí) 無序的描寫沒有經(jīng)驗(yàn) 還請各位大佬指點(diǎn)一番。 |

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鏈接: https://pan.baidu.com/s/1HqtSOpN8gBp_BvTsz4W8lg?pwd=i4je 提取碼: i4je 復(fù)制這段內(nèi)容后打開百度網(wǎng)盤手機(jī)App,操作更方便哦 僅供參考 #=============================================================================== #>>> The Following Improvement and Query ALERTS were generated - (Acta-Mode) <<< #=============================================================================== Format: alert-number_ALERT_alert-type_alert-level text 042_ALERT_1_C Calc. and Reported MoietyFormula Strings Differ Please Check 414_ALERT_2_C Short Intra D-H..H-X H1B ..H14 . 1.99 Ang. x,y,z = 1_555 Check 906_ALERT_3_C Large K Value in the Analysis of Variance ...... 2.586 Check #=============================================================================== 007_ALERT_5_G Number of Unrefined Donor-H Atoms .............. 3 Report 302_ALERT_4_G Anion/Solvent/Minor-Residue Disorder (Resd 2 ) 75% Note 912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 525 Note 933_ALERT_2_G Number of HKL-OMIT Records in Embedded .res File 1 Note 941_ALERT_3_G Average HKL Measurement Multiplicity ........... 2.8 Low 952_ALERT_5_G Calculated (ThMax) and CIF-Reported Lmax Differ. 3 Units 958_ALERT_1_G Calculated (ThMax) and Actual (FCF) Lmax Differ. 3 Units 978_ALERT_2_G Number C-C Bonds with Positive Residual Density. 8 Info #=============================================================================== |
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