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jinshanli至尊木蟲 (知名作家)
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[求助]
單晶有不少錯誤解析困難,請求幫助,謝謝!
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測出來的單晶有不少錯誤,說是單晶無序,請各位單晶解析高手幫忙解析一下,謝謝啦! 主要想確定結(jié)構(gòu)中標(biāo)紅的兩個基團(tuán)相對構(gòu)型,是順式還是反式的,非常感謝! |

專家顧問 (文壇精英)
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專家經(jīng)驗(yàn): +1066 |
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鏈接: https://pan.baidu.com/s/1Zb4qaDgj1s04-5GCbGqxLw 提取碼: yw9j 無序與否并不影響兩個目標(biāo)基團(tuán)位置的判斷 |

至尊木蟲 (正式寫手)
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test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level A EXPT005_ALERT_1_A _exptl_crystal_description is missing Crystal habit description. The following tests will not be performed. CRYSR_01 DIFF003_ALERT_1_A _diffrn_measurement_device_type is missing Diffractometer make and type. Replaces _diffrn_measurement_type. PLAT183_ALERT_1_A Missing _cell_measurement_reflns_used Value .... Please Do ! PLAT184_ALERT_1_A Missing _cell_measurement_theta_min Value ...... Please Do ! PLAT185_ALERT_1_A Missing _cell_measurement_theta_max Value ...... Please Do ! PLAT699_ALERT_1_A Missing _exptl_crystal_description Value ....... Please Do ! Alert level C PLAT041_ALERT_1_C Calc. and Reported SumFormula Strings Differ Please Check PLAT043_ALERT_1_C Calculated and Reported Mol. Weight Differ by .. 2.02 Check PLAT052_ALERT_1_C Info on Absorption Correction Method Not Given Please Do ! PLAT053_ALERT_1_C Minimum Crystal Dimension Missing (or Error) ... Please Check |

至尊木蟲 (正式寫手)
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test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level A EXPT005_ALERT_1_A _exptl_crystal_description is missing Crystal habit description. The following tests will not be performed. CRYSR_01 DIFF003_ALERT_1_A _diffrn_measurement_device_type is missing Diffractometer make and type. Replaces _diffrn_measurement_type. PLAT183_ALERT_1_A Missing _cell_measurement_reflns_used Value .... Please Do ! PLAT184_ALERT_1_A Missing _cell_measurement_theta_min Value ...... Please Do ! PLAT185_ALERT_1_A Missing _cell_measurement_theta_max Value ...... Please Do ! PLAT699_ALERT_1_A Missing _exptl_crystal_description Value ....... Please Do ! Alert level C PLAT041_ALERT_1_C Calc. and Reported SumFormula Strings Differ Please Check PLAT043_ALERT_1_C Calculated and Reported Mol. Weight Differ by .. 2.02 Check PLAT052_ALERT_1_C Info on Absorption Correction Method Not Given Please Do ! PLAT053_ALERT_1_C Minimum Crystal Dimension Missing (or Error) ... Please Check |

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