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聚合物木蟲 (著名寫手)
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[求助]
求助這樣的flack parameter是否可以說明單晶的絕對構(gòu)型是對的?@lich666 已有1人參與
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level c rinta01__3_c the value of rint is greater than 0.12 rint given 0.136 strva01__2_c chirality of atom sites is inverted? from the cif: _refine_ls_abs_structure_flack 1.024 from the cif: _refine_ls_abs_structure_flack_su 0.010 plat020__3_c the value of rint is greater than 0.12 ......... 0.136 report plat090__3_c poor data / parameter ratio (zmax > 18) ........ 7.20 note plat242__2_c low ’mainmol’ ueq as compared to neighbors of c30 check plat331__2_c small aver phenyl c-c dist c30 -c35 . 1.37 ang. plat410__2_c short intra h...h contact h1 ..h8 . 1.94 ang. x,y,z = 1_555 check plat907__2_c flack x > 0.5, structure needs to be inverted? . 1.02 check plat987__1_c the flack x is >> 0 - do a basf/twin refinement please check 求助這個(gè)單晶是否可以說明其絕對構(gòu)型是對的? |

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